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The influence of spark plasma sintering temperatures on the microstructure,hardness,and elastic modulus of the nanocrystalline Al-xV alloys produced by high-energy ball milling

查看全文 作  者:[1]J.Christudasjustus;[1]C.S.Witharamage;Ganesh [2]Walunj;[2]T.Borkar;[1]R.K.Gupta 高影响力作者 机构地区:[1]Department of Materials Science and Engineering,North Carolina State University,Raleigh,NC 27606,United States;[2]Department of Mechanical Engineering,Cleveland State University,Cleveland,OH 44115,United States高影响力机构 出  处:《Journal of Materials Science & Technology》索引2022年第27期,共9页高影响力期刊 基  金:the financial support received from the National Science Foundation(Nos.NSF-CMMI 1760204 and 2131440)under the direction of Dr.Alexis Lewis;supported by the State of North Carolina and the National Science Foundation(No.ECCS-1542015);support from the National Science Foundation(DMR1726294)。 摘  要:Al-xV alloys(x=2 at.%,5 at.%,10 at.%)with nanocrystalline structure and high solid solubility of V were produced in powder form by high-energy ball milling(HEBM).The alloy powders were consolidated by spark plasma sintering(SPS)employing a wide range of temperatures ranging from 200 to 400°C.The microstructure and solid solubility of V in Al were investigated using X-ray diffraction analysis,scanning electron microscope and transmission electron microscope.The microstructure was influenced by the SPS temperature and V content of the alloy.The alloys exhibited high solid solubility of V–six orders of magnitude higher than that in equilibrium state and grain size<50 nm at all the SPS temperatures.The formation of Al3V intermetallic was detected at 400℃.Formation of a V-lean phase and bimodal grain size was observed during SPS,which increased with the increase in SPS temperature.The hardness and elastic modulus,measured using nanoindentation,were significantly higher than commercial alloys.For example,Al-V alloy produced by SPS at 200℃ exhibited a hardness of 5.21 GPa along with elastic modulus of 96.21 GPa.The evolution of the microstructure and hardness with SPS temperatures has been discussed. 关 键 词:Spark plasma sintering Aluminum alloys Nanocrystalline alloys High-energy ball milling NANOINDENTATION HARDNESS Elastic modulus
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