Synthesis and Characterizations of Nanocrystalline WC-Co Composite Powders by a Unique Ball Milling Process

查看全文 作　　者：Jun SHEN, Jianfei SUN and Faming ZHANGSchool of Materials Science and Engineering, Harbin Institute of Technology, Harbin 150001, China

出　　处：《Journal of Materials Science & Technology》索引2004年第20卷第1期,共4页

摘　　要：In order to explore the high efficiency of fabricating nanocrystalline WC-Co composite powders, this paper presented a unique high energy ball milling process with variable rotation rate and repeatious circulation, by which nanocrystalline WC-10Co0.8VC-0.2Cr3C2 (wt pct) composite powders with mean grain size of 25 nm were prepared in 32 min, and the quantity of the powders for a batch was as much as 800 grams. The as-prepared powders were analyzed and characterized by chemical analysis,X-ray diffraction (XRD), transmission electron microscopy (TEM) and differential thermal analysis (DTA). The results show that high energy ball milling with variable rotation rates and repeatious circulation could be used to produce nanocrystalline WC-Co powder composites with high efficiency. The compositions of the powders meet its specifications with low impurity content. The mean grain size decreases, lattice distortion and system energy increase with increasing the milling time. The morphology of nanocrystalline WC-Co particles displays dominantly sphere shape and their particle sizes are all lower than 80nm. The eutectic temperature of the nanocrystalline WC-10Co-0.8VC-0.2Cr3C2 composites is about 1280℃. 关键词：纳米晶体材料 WC-Co复合粉末球磨研磨技术 X射线衍射钴

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Synthesis and Characterizations of Nanocrystalline WC-Co Composite Powders by a Unique Ball Milling Process

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耦合文献(35)

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